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1100 Series Capillary LC System Manual 19
Installing your Capillary LC System 1
Install the Capillary Pump (G1376A)
1 Ensure the line power switch at the front of the capillary pump is off.
2 Place the capillary pump on the bench, positioned to the left of the micro
sampler thermostat module.
3 Connect the power cable to the power socket at the rear of the capillary
pump. Do not connect the power cable to power until you have finished the
hardware installation of all modules in the stack.
4 Connect the 1-meter CAN-bus cable (5181-1519) from one of the CAN-bus
connectors at the rear of the capillary pump to the free CAN-bus connector
at the rear of the micro sampler.
5 Connect the pre-terminated end of the pump-to-sampler capillary
(G1375-87310) to the flow sensor outlet of the pump. Connect the other end
of this capillary to port 1 of the micro sampler injection valve.
6 Connect the 1/8 inch plastic EMPV waste tube to the barbed waste fitting of
the EMPV. Route the waste tube to an appropriate waste container.
7 Connect the large-bore corrugated plastic leak drain tubing to the pump
leak drain fitting. Route the leak drain tubing to an appropriate waste
container.
WARNING
Connect the power cable to power only after you have finished the hardware
installation of all modules in the stack.
NOTE
Carefully route all capillaries so that they are not crushed or broken by module front covers.
Avoid excessive bending. See Chapter 2 for advice on handling capillaries.
- Agilent 1100 Series 1
- Capillary LC System 1
- In This Manual… 3
- Contents 5
- Agilent Technologies 11
- Site Requirements 12
- Bench Space 13
- Environment 13
- Physical Specifications 14
- System Installation Process 16
- Install the Solvent Cabinet 23
- Micro Well-plate Sampler) 26
- Purging the Pump 34
- Inject the Check-out Sample 36
- Procedure 37
- Optimizing Performance 39
- Pump issues 40
- Fused Silica Capillary issues 41
- Sampler issues 42
- Column thermostat issues 42
- DAD issues 42
- Cleaning the Solvent Filters 45
- When to use Alternative Seals 47
- Static Mixer and Filter 50
- How the Function Works 53
- Capillaries and Fittings 55
- Capillary Flow Diagram 56
- Capillaries and Fittings 3 57
- * 2.2 12 5065-9906 61
- * 1.4 7.6 G1375-87313 61
- Fittings and Ferrules 62
- Basic System Troubleshooting 65
- Symptoms: 66
- Poor peak shape 71
- Wandering Detector Baseline 73
- Parts and Materials 75
- Micro Vacuum Degasser 76
- Capillary Pump 79
- Capillary Pump Hydraulic Path 82
- Pump-Head Assembly 84
- Figure 9 Pump head assembly 85
- Capillary pump cover parts 86
- Micro Well-plate Sampler 87
- Thermostat for 1100 Samplers 98
- 5 Parts and Materials 100
- Parts and Materials 5 101
- Vial Trays 104
- Micro Column Switching Valve 107
- Diode Array Detector 111
- DAD - Optical Unit Assembly 113
- Figure 30 Optical Unit Parts 114
- 500 nl Flow Cell 115
- Fan Assembly Parts 117
- Holmium Oxide Filter 118
- Common Parts 120
- Rear panel 121
- Power and Status Light Pipes 122
- Leak Parts 123
- Foam parts 124
- Sheet metal kit 124
- Micro Degasser Accessory Kit 125
- Capillary Pump Accessory Kit 126
- G1316-68725 129
- DAD Accessory Kit 130
- Tabl e 61 Cables overview 131
- Analog Cables 133
- Remote Cables 134
- BCD Cables 140
- Auxiliary Cable 142
- CAN Cable 142
- External Contact Cable 143
- RS-232 Cable Kit 144
- LAN Cables 144
- Options 6 147
- 6Options 152
- Frequency If valve leaks 156
- 9/64 inch hex key 156
- • Disconnect the power cable 157
- • Disconnect capillaries 157
- Features 163
- Performance Specification 163
- Installation of the Flow Cell 166
- ~ 0.3 mm clearance 167
- Replacing or Cleaning Parts 171
- Performance Specifications 175
- 7 Performance Specifications 176
- Performance Specifications 7 177
- Autosampler 179
- Compartment 181
- Safety Information 185
- Operation 186
- Safety Symbols 187
- Lithium Batteries Information 188
- Danish Information: 188
- Radio Interference 189
- Sound Emission 189
- Solvent Information 189
- ' %%(&' 196
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