Agilent Technologies 1100 Series Betriebsanweisung

Agilent TechnologiesAgilent 1100 Series Valves User’s Guide

4 Agilent 1100 Series Valves1 Installation and ConfigurationUnpacking the 1100 Series ValveThe M4 micro valve fittings support the Agilent PEEK coated

Agilent 1100 Series Valves 5Installation and Configuration 1Hardware InstallationHardware InstallationThe Agilent 1100 Series External Valves can be i

6 Agilent 1100 Series Valves1 Installation and ConfigurationHardware InstallationIn order to install a valve on the G1383A Column Organizer the Organi

Agilent 1100 Series Valves 7Installation and Configuration 1Hardware InstallationSetting up the power connection to other Agilent 1100 Series ModulesT

8 Agilent 1100 Series Valves1 Installation and ConfigurationSoftware ConfigurationSoftware ConfigurationThe 1100 Series Valves can be controlled by th

Agilent 1100 Series Valves 9Installation and Configuration 1Software ConfigurationFigure 3 Valve configuration

10 Agilent 1100 Series Valves1 Installation and ConfigurationSoftware Configuration

11Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies2OperationOperating the Valve using Agilent ChemStation 12Handheld Controller

12 Agilent 1100 Series Valves2OperationOperating the Valve using Agilent ChemStationOperating the Valve using Agilent ChemStationAfter the Agilent 110

Agilent 1100 Series Valves 13Operation 2Operating the Valve using Agilent ChemStationAfter the run is finished, the valve always switches to the start

Agilent 1100 Series ValvesNotices© Agilent Technologies, Inc. 2002, 2004No part of this manual may be reproduced in any form or by any means (includin

14 Agilent 1100 Series Valves2OperationOperating the Valve using Agilent ChemStationPosition DescriptionsDefine the Position Description that is used

Agilent 1100 Series Valves 15Operation 2Operating the Valve using Agilent ChemStationNext position after runIf Next position after run is checked, the

16 Agilent 1100 Series Valves2OperationHandheld Controller functionsHandheld Controller functionsWith firmware revision B.03.11 or higher the followin

Agilent 1100 Series Valves 17Operation 2Handheld Controller functionsSetting the EMF limit and switch counter1 From the startup screen of the Agilent

18 Agilent 1100 Series Valves2OperationHandheld Controller functions

19Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies3Maintenance, Repair, and TroubleshootingStatus Indicators 20Maintenance and

20 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingStatus IndicatorsStatus IndicatorsThe instrument status indicator indicates one

Agilent 1100 Series Valves 21Maintenance, Repair, and Troubleshooting 3Maintenance and RepairMaintenance and RepairThe maintenance of the Agilent 1100

22 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingMaintenance and RepairReplacing the stator face and the rotor seal for standard

Agilent 1100 Series Valves 23Maintenance, Repair, and Troubleshooting 3Maintenance and Repair2 Align the Stator Ring (4) that the two short pins on th

Agilent 1100 Series Valves iiiIn This Guide…The Agilent 1100 Series valves provide the user a comprehensive solutions for more flexibility through sol

24 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingMaintenance and RepairReplacing the rotor seal for micro valves (G1162A and G11

Agilent 1100 Series Valves 25Maintenance, Repair, and Troubleshooting 3Maintenance and RepairReassembling the valve head1 Mount the new Rotor Seal (5)

26 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingMaintenance and Repair• Stator heads Stator head for G1157 (2 position/10 port

Agilent 1100 Series Valves 27Maintenance, Repair, and Troubleshooting 3Maintenance and RepairEarly Maintenance Feedback (EMF)Depending on the applicat

28 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingMaintenance and RepairResetting the EMF counter1 Switch to the Diagnostics View

Agilent 1100 Series Valves 29Maintenance, Repair, and Troubleshooting 3System Errors and TroubleshootingSystem Errors and TroubleshootingSystem Errors

30 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingSystem Errors and TroubleshootingCAN failureError Cause If the red Pow. fail st

Agilent 1100 Series Valves 31Maintenance, Repair, and Troubleshooting 3System Errors and TroubleshootingUnknown PositionError Cause An unknown positio

32 Agilent 1100 Series Valves3 Maintenance, Repair, and TroubleshootingSystem Errors and TroubleshootingValve SynchronizationIf the valve failed to sw

33Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies4Valve ApplicationsAlternating Column Regeneration 34Sample enrichment and Sa

iv Agilent 1100 Series ValvesChapter 3, “Maintenance, Repair, and Troubleshooting,” starting on page 19 will describe recommended maintenance and repa

34 Agilent 1100 Series Valves4 Valve ApplicationsAlternating Column RegenerationAlternating Column RegenerationAlternating column regeneration is a co

Agilent 1100 Series Valves 35Valve Applications 4Alternating Column RegenerationIf the valve is switched to position 1 the eluent pump delivers the mo

36 Agilent 1100 Series Valves4 Valve ApplicationsAlternating Column RegenerationCapillary Kit (G1156-68711) for alternating column regeneration with G

Agilent 1100 Series Valves 37Valve Applications 4Alternating Column RegenerationCapillary Kit (G1156-68713) for alternating column regeneration with G

38 Agilent 1100 Series Valves4 Valve ApplicationsSample enrichment and Sample strippingSample enrichment and Sample strippingSample enrichment and sam

Agilent 1100 Series Valves 39Valve Applications 4Sample enrichment and Sample strippingFor the sample enrichment phase the valve is switched to positi

40 Agilent 1100 Series Valves4 Valve ApplicationsSample enrichment and Sample strippingFigure 22 on page 39 illustrates how the Agilent 1100 Series 2

Agilent 1100 Series Valves 41Valve Applications 4Sample enrichment and Sample strippingTabl e 12 Fittings, screws, and ferrulesDescription Qty part nu

42 Agilent 1100 Series Valves4 Valve ApplicationsColumn SelectionColumn SelectionWith the Agilent 1100 Series 6 position selection valve (G1159A) and

Agilent 1100 Series Valves 43Valve Applications 4Column SelectionCapillary Kit (G1156-68712) for column selection with G1159A (analytical scale)Tabl e

contentsAgilent 1100 Series Valves iContents1 Installation and ConfigurationSite Requirements 2Unpacking the 1100 Series Valve 3Damaged Packaging 3Del

44 Agilent 1100 Series Valves4 Valve ApplicationsSolvent SelectionSolvent SelectionThe 1100 Series 12 position / 13 port valve can be used for solvent

Agilent 1100 Series Valves 45Valve Applications 4Solvent SelectionTubing Kit (G1160-68706) for solvent selection (4 solvents) with G1160A, degasser an

46 Agilent 1100 Series Valves4 Valve ApplicationsSolvent Selection

47Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies5PartsGeneral Parts 48Capillaries and Fittings for analytical and preparative

48 Agilent 1100 Series Valves5PartsGeneral PartsTabl e 17 General partsDescription part number• CAN cable, 1m long 5181-1519• DC-Can cable 5181-1533•

Agilent 1100 Series Valves 49Parts 5Tabl e 19 Rebuild kits and repair parts for Agilent 1100 Series ValvesDescription part number• Rebuilt kits and ro

50 Agilent 1100 Series Valves5PartsCapillaries and Fittings for analytical and preparative flow ratesTabl e 20 Capillary and tubing kitsDescription pa

Agilent 1100 Series Valves 51Parts 5Capillaries and Fittings for micro valvesFor the operation of the Agilent 1100 Series Micro Valves we recommend th

52 Agilent 1100 Series Valves5PartsTabl e 23 Fitting TypesFittings and ferrules Fitting typeABCDTabl e 24 PEEK coated fused silica capillaries for mic

Agilent 1100 Series Valves 53Parts 550 220 0.432 B/B G1375-8730150 280 0.550 C/D G1375-8730950 400 0.785 E/D G1315-6870350 500 0.982 C/D G1375-8730450

ii Agilent 1100 Series Valvescontents4 Valve ApplicationsAlternating Column Regeneration 34Sample enrichment and Sample stripping 38Sample enrichment

54 Agilent 1100 Series Valves5Parts

55Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies6SpecificationsG1157A Agilent 1100 Series 2 position / 10 port valve 56G1158A

56 Agilent 1100 Series Valves6 SpecificationsTabl e 25 G1157A Agilent 1100 Series 2 position / 10 port valveLiquid contacts: Stainless Steel and PEEKP

Agilent 1100 Series Valves 57Specifications 6* The G1159A 1100 Series 6 positions selection valve can be used at flow rates up to 100 ml/min, but with

58 Agilent 1100 Series Valves6 SpecificationsVolume in flow passages: Stator (20° ports)27.2 nl, (45° ports) 30.5 nl, rotor seal 25.0 nl/grooveMaximum

59Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies7Safety InformationGeneral Safety Information 60Lithium Batteries Information

60 Agilent 1100 Series Valves7 Safety InformationGeneral Safety InformationGeneral Safety InformationThe following general safety precautions must be

Agilent 1100 Series Valves 61Safety Information 7General Safety Informationattempt internal service or adjustment unless another person, capable of re

62 Agilent 1100 Series Valves7 Safety InformationGeneral Safety InformationSafety SymbolsTable 31 shows safety symbols used on the instrument and in t

Agilent 1100 Series Valves 63Safety Information 7Lithium Batteries InformationLithium Batteries InformationWARNINGDanger of explosion if battery is in

1Agilent 1100 Agilent 1100 Series ValvesUser’s GuideAgilent Technologies1Installation and ConfigurationSite Requirements 2Unpacking the 1100 Series Va

64 Agilent 1100 Series Valves7 Safety InformationRadio InterferenceRadio InterferenceNever use cables other than the ones supplied by Aligent Technolo

Agilent 1100 Series Valves 65Safety Information 7Sound EmissionSound EmissionManufacturer’s DeclarationThis statement is provided to comply with the r

66 Agilent 1100 Series Valves7 Safety InformationSolvent InformationSolvent InformationObserve the following recommendations on the use of solvents.So

Agilent 1100 Series Valves 67Safety Information 7Agilent Technologies on InternetAgilent Technologies on InternetFor the latest information on product

68 Agilent 1100 Series Valves7 Safety InformationAgilent Technologies on Internet

Agilent 1100 Series Valves 69IndexAaccessory kit, 3Agilent ChemStation, 8, 12Agilent on internet, 67alternating column regeneration, 34analytical scal

70 Agilent 1100 Series ValvesIndexstator ring, 22, 24Status Indicators, 20switch failure, 30switching the valve, 16synchronization, 16, 32system error

 Agilent Technologies 2002, 2004Printed in Germany 09/2004*G1156-90001**G1156-90001*G1156-90001www.agilent.comAgilent TechnologiesIn This BookThis Us

2 Agilent 1100 Series Valves1 Installation and ConfigurationSite RequirementsSite RequirementsThe requirements for the Agilent 1100 Series Valves are

Agilent 1100 Series Valves 3Installation and Configuration 1Unpacking the 1100 Series ValveUnpacking the 1100 Series ValveDamaged PackagingIf the deli