Agilent Technologies 5975 Spezifikationen

Agilent Technologies5975 Series Mass Selective DetectorsHardware Installation

10 Hardware Installation1 General InformationFigure 1 5975 Series MSD systemALS7890A GCCI gas flow moduleLocal control panel5975 Series MSDMSD power s

General Information 1Hardware Installation 11Important Safety WarningsBefore moving on, there are several important safety notices that you should alw

12 Hardware Installation1 General InformationMany parts are dangerously hotMany parts of the MSD operate at temperatures high enough to cause serious

General Information 1Hardware Installation 13When using hydrogen gas, check the system for leaks to prevent possible fire and explosion hazards based

14 Hardware Installation1 General InformationSafety and Regulatory CertificationsThe 5975 Series Mass Selective Detector conforms to the following saf

General Information 1Hardware Installation 15Refer servicing to qualified service personnel. Substituting parts or performing any unauthorized modific

16 Hardware Installation1 General InformationElectromagnetic compatibilityThis device complies with the requirements of CISPR 11. Operation is subject

General Information 1Hardware Installation 17CleaningTo clean the unit, disconnect the power and wipe down with a damp, lint-free cloth.Recycling the

18 Hardware Installation1 General InformationCustomer ResponsibilitiesThe following are not included in the standard installation. They are the respon

General Information 1Hardware Installation 19Before You StartVerify that all the conditions specified in the 5975 Series MSD Site Preparation Guide ha

2 Hardware InstallationNotices© Agilent Technologies, Inc. 2010No part of this manual may be reproduced in any form or by any means (including elec-tr

20 Hardware Installation1 General InformationOther DocumentationAdditional information is contained in the following documentation:• 5975 Series Mass

215975 Series Mass Selective DetectorsHardware InstallationAgilent Technologies2InstallationOverview 22Unpacking and Inspecting the Materials 2

22 Hardware Installation2 InstallationOverview Listed below are the steps performed for hardware installation. The actual order of the steps depends u

Installation 2Hardware Installation 23Unpacking and Inspecting the MaterialsShipping containers should not be opened until an Agilent Technologies rep

24 Hardware Installation2 InstallationInstalling the GCMaterials needed:Column cutter (5181-8836) Flat-blade screwdriver GC Series shipping kitPlease

Installation 2Hardware Installation 25Figure 3 Removing the knockoutsMetal knockoutsGC/MSD interface heater cable (GC end)

26 Hardware Installation2 InstallationConnecting the Helium Lines to the GC1 Connect the 6-foot copper tubing (or a custom length) to the carrier gas

Installation 2Hardware Installation 27Purge the flow system for 20 minutes. You can continue with the next step while you wait.

28 Hardware Installation2 InstallationConfiguring the GC1 If there is an ALS, install it now. Follow the instructions provided with the ALS. 2 Install

Installation 2Hardware Installation 29Conditioning the Column1 Remove the septum covering the free end of the GC column and cut about 1 cm off the end

Hardware Installation 3Contents1 General InformationIntroduction 8Important Safety Warnings 11Many internal parts of the MSD carry dangerous

30 Hardware Installation2 InstallationPreparing the MSD for InstallationMaterials needed:5975 Series MSD Hardware Manual Tygon tubing or hose for pump

Installation 2Hardware Installation 31Preparing the Vacuum SystemMaterials needed:5975 Series MSD Hardware Manual Diagonal cutters Plastic gloves1 Rem

32 Hardware Installation2 Installation6 Remove the blank flange from the free end of the hose, and connect the hose to the inlet port of the pump. 7 I

Installation 2Hardware Installation 339 Install the optional G3397A High vacuum gauge controller (required for CI MSDs). Be sure not to stress the cab

34 Hardware Installation2 InstallationPlumbing the Methane Line to the CI MSD Flow ModuleSpecial procedure for CI MSDRefer to the 5975 Series MSD Hard

Installation 2Hardware Installation 357 Let the lines purge into a fume hood for 5 to 10 minutes.8 Connect the other end of the tubing to the Gas A fi

36 Hardware Installation2 InstallationConnecting the MSD and the GC1 Verify that the GC power is turned off.2 Connect the two ends of the GC/MSD inter

Installation 2Hardware Installation 37When positioned properly, the end of the GC/MSD interface cover will touch the metal of the oven wall, and the e

38 Hardware Installation2 InstallationPress on the side plate of the MSD to achieve a good seal. Verify that the foreline pump and the front fan turn

Installation 2Hardware Installation 39Installing the ChemStation PC 1 Unpack the PC, monitor, printer, and the modem (if present).2 Position the PC co

4 Hardware InstallationConditioning the Column 29Preparing the MSD for Installation 30Preparing the Vacuum System 31Plumbing the Methan

40 Hardware Installation2 InstallationVerifying EI System PerformanceMaterial needed:1 pg/µL (0.001 ppm) OFN sample (5188-5348)Verify the tune perform

Installation 2Hardware Installation 41Switching from EI to CI Operating ModeSpecial procedure for CI MSDRefer to the 5975 Series MSD Hardware Manual.1

42 Hardware Installation2 InstallationVerifying CI System PerformanceSpecial procedure for CI MSDRefer to the 5975 Series MSD Hardware Manual.Verify P

Installation 2Hardware Installation 43Verifying High Mass System PerformanceRefer to the 5975 Series MSD Hardware Manual.To check high mass performanc

44 Hardware Installation2 InstallationFamiliarizing the CustomerFollow the “Customer Familiarization Checklist” on page 53.Important points about the

455975 Series Mass Selective DetectorsHardware InstallationAgilent Technologies3ChecklistsInstallation Checklist 46Customer Familiarization Checkl

46 Hardware Installation3 ChecklistsInstallation ChecklistVerifying that site preparation is complete Adequate space is available for the MSD system.

Checklists 3Hardware Installation 47 Shipment damaged or incomplete:GC installation The following steps are general, and may differ slightly dependin

48 Hardware Installation3 Checklists GC plumbedConfiguring the GC ALS installed (optional) Merlin Microseal installed (optional)  GC plugged in an

Checklists 3Hardware Installation 49 PFDTD vial for CI cal valve filledPreparing the vacuum system Plugs removed from the foreline pump Foreline pu

Hardware Installation 5MSD ChemStation software overview 54MSD ChemStation software autotune descriptions 54Methods 55Data acquisition

50 Hardware Installation3 Checklists Foreline pump and the front fan operation verified Foreline pump stops gurgling within 60 seconds verified MSD

Checklists 3Hardware Installation 51 EI ion source removed CI ion source installed CI interface tip seal installed MSD pumped down and baked out f

52 Hardware Installation3 ChecklistsInstrument Log Book updated MSD serial number recorded on S/N report S/N Report(s) and Tune Report(s) faxed to G

Checklists 3Hardware Installation 53Customer Familiarization ChecklistThe purpose of customer familiarization is to demonstrate the steps required to:

54 Hardware Installation3 ChecklistsHardware overview MSD CI MSD (if applicable) Gas Chromatograph ALS (if applicable) Bar code reader (if applic

Checklists 3Hardware Installation 55 Manual tune explained View Tunes utility demonstrated and its importance explained PCI Autotune performed (if

56 Hardware Installation3 Checklists Library search (searching a spectrum) demonstrated Difference between standalone and online data analysis expla

Checklists 3Hardware Installation 57 Differences between the EI and CI source parts described Differences in installation and removal of the EI vers

58 Hardware Installation3 ChecklistsCompany name:Sales order number:Customer signature/date:Engineer signature/date:

6 Hardware Installation

Agilent Technologies© Agilent Technologies, Inc. Printed in USA, March 2010G3170-90002

75975 Series Mass Selective DetectorsHardware InstallationAgilent Technologies1General InformationIntroduction 8Important Safety Warnings 11Saf

8 Hardware Installation1 General InformationIntroductionThis document provides installation instructions for the Agilent Technologies 5975 Series Mass

General Information 1Hardware Installation 9Table 1 Available high vacuum pumpsModel name Product number Description Ionization modes5975C TAD VL M